Search results for "Bile acid precursor"

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International descriptive and interventional survey for oxycholesterol determination by gas- and liquid-chromatographic methods

2018

International audience; Increasing numbers of laboratories develop new methods based on gas-liquid and high-performance liquid chromatography to determine serum concentrations of oxygenated cholesterol metabolites such as 7alpha-, 24(S)-, and 27-hydroxycholesterol. We initiated a first international descriptive oxycholesterol (OCS) survey in 2013 and a second interventional survey 2014 in order to compare levels of OCS reported by different laboratories and to define possible sources of analytical errors. In 2013 a set of two lyophilized serum pools (A and B) was sent to nine laboratories in different countries for OCS measurement utilizing their own standard stock solutions. In 2014 eleven…

0301 basic medicineHigh performance-liquid chromatography[SDV.BIO]Life Sciences [q-bio]/BiotechnologyChromatography GasDeuterium labelledHigh-performance liquid chromatographyBiochemistryBile acid precursor03 medical and health sciencesOxysterolgasSurveys and QuestionnairesHumansSurveys and QuestionnaireliquidReference standardsbile acid precursors; gas-liquid chromatography; high performance-liquid chromatography; isotope dilution; mass spectrometry; oxysterol; cholesterol; chromatography gas; chromatography liquid; humans; reference standards; surveys and questionnaires; biochemistryChromatographyMass spectrometry[CHIM.ORGA]Chemical Sciences/Organic chemistryBile acid precursorsChromatography liquidGeneral MedicineStandard methodsSerum concentrationReference Standards16. Peace & justiceIsotope dilution3. Good health030104 developmental biologyGas-liquid chromatographyCholesterolChromatography GaEnvironmental sciencechromatographyReference StandardGas chromatographybile acid precursorsChromatography LiquidHuman

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